Síntesis y caracterización del superconductor Eu3Ba5Cu8O18-δ dopado con 0.1% de óxido de Grafeno

Synthesis and characterization of Eu3Ba5Cu8O18-δ superconductor doped with 0.1% Graphene oxide

Published 2024-07-01

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Vol. 21 No. 42 (2024): Estructura cristalina del superconductor
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Síntesis y caracterización del superconductor Eu3Ba5Cu8O18-δ dopado con 0.1% de óxido de Grafeno. (2024). Revista EIA, 21(42), 4201 pp. 1-20. https://doi.org/10.24050/reia.v21i42.1785
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Sully Segura Peña
Universidad de Oviedo. Asturias
Luis Fernando Parra Suarez
Universidad Santo Tomás, Colombia
Laura Natalia Ayala Sotelo
Universidad Santo Tomás, Colombia
Maria Rosario Maldonado Cardenas
Universidad Santo Tomás, Colombia
Julian David Segura Peña
Universidad Santo Tomás, Colombia
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Esta investigación presenta la síntesis y evaluación de las propiedades estructurales y morfológicas del superconductor Eu3Ba5Cu8O18-δ dopado con un 0.1% de óxido de grafeno, utilizando el método de reacción de estado sólido. El análisis estructural realizado en las muestras, tanto en la no dopada como en la dopada, permitió identificar la fase principal como Eu3Ba5Cu8O18-δ (Eu358), con estructura ortorrómbica y grupo espacial Pmm2(25), manteniendo propiedades superconductoras en ambos casos. Además, se observó que el dopaje con óxido de grafeno dio lugar a la formación de una fase minoritaria de EuBa4Cu3O9 (Eu143), con estructura cúbica y grupo espacial P23(195). En cuanto a la caracterización morfológica, se evidenció que la muestra no dopada presenta agregados conformados por granos de tamaño no uniforme, con un tamaño medio con un tamaño medio de aproximadamente 97 µm. En contraste, la muestra dopada con un 0.1% de óxido de grafeno exhibe mejoras significativas en la uniformidad y límites de los granos, con un tamaño medio de alrededor de 141 µm. Estos resultados confirman la obtención de Eu3Ba5Cu8O18-δ con una fase superconductora del 73%, superando los porcentajes reportados previamente utilizando el método de reacción de estado sólido.

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